Thermal evaporation is a simple method of physical vapor deposition. It is a high-vacuum technology for depositing thin films of materials on the surface of various substrates. The thickness of the films is usually in the order of a few Å to several hundred nm. The technique involves heating a solid source material until a certain vapor pressure is produced. The evaporated material then reaches the substrate and sticks to it, creating the required coating. The material is evaporated by Joule (resistive) heating, by passing a high current through a thin resistive boat, crucible, coil or filament usually made of W, Ta or Mo, depending on the material to be evaporated. Usually two or more materials can be evaporated in the same pump down, without breaking the vacuum. A wide variety of materials can be deposited, both metals and nonmetals, such as Al, Ag, Ni, Cr,Au, In, among many other materials, whose vapor pressure can be reasonable at a temperature of 1600 oC or below. Thermal evaporation can usually achieve very high deposition rates (up to 50 Å/s). The thickness of the deposited film can be precisely monitored in-situ using a quartz balance.
Thermal evaporation can be used for blanket depositions, it can be combined with a lithographic technique either in a lift-off or an etching process or, for larger patterns, it can also be performed through a shadow mask. Thermal evaporation is compatible with most substrates and resists. Often the deposition can be combined with a tilted or a rotating substrate (or both). Thermal evaporation is not appropriate for applications where good step coverage is necessary or for high purity films, where other techniques are more appropriate. However it is a quick and simple method for a variety of applications, e.g. for defining metallic alignment markers, metallic etch masks, simple electrical contacts, electroplating seed layers etc.
In SEM a beam is scanned over a sample surface while a signal from secondary or back-scattered electrons is recorded. SEM is used to image an area of the sample with nanometric resolution, and also to measure its composition, crystallographic phase distribution and local texture.
Laser patterning is a technique for the controlled patterning of materials at micro- and nano-scales. It offers the ability to directly write patterns on the surface and complex 3D channels into the bulk of solid materials, also biomaterials. Applications can range from microfluidic systems and sensors to tissue engineering scaffolds.
Electron-beam lithography is a direct write nanopatterning technique utilizing a finely focused electron beam in order to write nanoscale patterns on special e-beam resists in two and three dimensions. Compared to other nanostructuring methods, it stands out for its high level of flexibility and resolution and reasonable patterning speed.
RIE is used to etch various materials under vacuum in the presence of reactive ions. The sample to be etched is placed in a vacuum chamber and gas is injected into the process chamber via a gas inlet in the top electrode. The lower electrode is negatively biased and a single RF plasma source determines both the ion density and their energy.
Ultraviolet lithography also known as optical or photolithography is the most commonly used patterning technique in microfabrication. A photosensitive material (photoresist) is spin-coated onto the substrate to be patterned. The photoresist is illuminated with UV light through a photomask which contains the relevant geometric patterns.